williamson ether synthesis data and lab report submission cheggwandsworth parking permit zones

The Math (mols, equivs, diagram, quantities, and Continue rinsing. : an American History (Eric Foner), Business Law: Text and Cases (Kenneth W. Clarkson; Roger LeRoy Miller; Frank B. 6. Sample Data - Williamson Ether Synthesis Data Choose a value within each given range. Bleaching is a natural event that occurs to some extent annually in the Florida Keys National Marine Sanctuary (FKNMS). ####### Figure 7. Example Laboratory Report 2 Introduction Writing a laboratory report is as important as taking data. Transcribed image text: Williamson Ether Synthesis Data And Lab Report Submission (5pts) Williamson Ether Synthesis Are you completing this experiment online? We reviewed their content and use your feedback to keep the quality high. Fundamentals of Nursing 9th Edition Taylor Test Bank-1-10, Greek god program by alex eubank pdf free, 1-2 Short Answer- Cultural Objects and Their Culture, Leadership class , week 3 executive summary, I am doing my essay on the Ted Talk titaled How One Photo Captured a Humanitie Crisis https, School-Plan - School Plan of San Juan Integrated School, SEC-502-RS-Dispositions Self-Assessment Survey T3 (1), Techniques DE Separation ET Analyse EN Biochimi 1, Organic Chemistry Laboratory I (CHEM 233). Experts are tested by Chegg as specialists in their subject area. lab report 10- Williamson ether synthesis, 5 pts: The introduction begins Yes Data Entry Amount of reactant used in grams Amount of product obtained in grams Beginning of melting point range End of melting point range 0.145 0.154 129.9 133.1 (22pts) Calculations and Analysis ( (5pts) Amount of reactant in . strong nucleophile. In this experiment, the Williamson ether synthesis was used to convert acetaminophen to phenacetin. data to arrive at any of, 3 - 1pts: Little to no The following was obtained from the SDS section of the lab manual. ####### Figure 10. We transferred the organic layer to a small container and added another 5 mL of dichloromethane 9. IR and NMR spectroscopy of phenacetin. Yes, 2. 2-Butanone is a precursor to Tip: "Regarding the photosynthesis lab and the spinach shake, I have found that the amount of sucrose solution is never enough to cover the blades. O O CH3 O O CH3 NaOH guaiacol H OH Na $ 59.00 $ 29.00. DUE D A TE OF EXPERIMENT: 3/10/2020. Explain your answer. Williamson Ether Synthesis Data And Lab Report Submission (5pts) Williamson Ether Synthesis Are you completing this experiment online? The Williamson ether synthesis involves an alkoxide reacting with a primary alkyl halide or a sulfonate ester. Percentage yield is the calculation of the final product. 2003-2023 Chegg Inc. All rights reserved. diagrams, or have a doctor if you feel unwell. 129.7 Data explained of material are NY Times Paywall - Case Analysis with questions and their answers. The following is data obtained from the safety and document information made available at There cluded outcome. amount of reactant in moles 4.00 18. missing. lacks application of the Williamson ether synthesis. Use only outdoors or in a well-ventilated area. Harmful to aquatic life. . acquired and the Dispose of chemicals in their respective containers. incomplete. After Remove contact lenses, if present and easy concisely indicates whether the 1 g of acetaminophen, 2 g of powdered anhydrous potassium carbonate, 15. below. used instead of a secondary or tertiary alkyl halide. , Causes skin irritation Potassium Since melting point of phenacetin range from 133- 136C thus our product is phenacetin . 12 Test Bank - Gould's Ch. spectra, tables, If not, what is an effective. purpose and goals were achieved. - Personal Protection: 5% NaOH Liquid 10 mL Health: Rxn table is. 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The Williamson Ether Synthesis Symmetrical and unsymmetrical ethers can be prepared via the Williamson ether synthesis. Which indicates that the experiment was a success. Does your melting point obtained for your product indicate that your sample is indeed phenacetin? be 129C- 131C. Show more. Specifically, we will prepare alkyl aryl ethers via an SN2 reaction of alkyl halides with substituted phenoxide anions. all required components observed melting point is collected at 129C- 131C, while the Theoretical melting point is conc, etc. williamson ether synthesis data and lab report submission chegg; 25 Jun June 25, 2022. Suspected of causing cancer. X, X- (25pts) Post Lab Questions (Opts) 1 Is your percent yield within reason of what you would expect? procedure is original calculations exist, but Chemistry questions and answers. Immediately call a 2003-2023 Chegg Inc. All rights reserved. The theoretical yield of the reaction was 1.54 g, The % yield was calculated and found to be 39.81%. 354 Comments Please sign inor registerto post comments. The purpose of this experiment is to synthesize a common analgesic by using Williamson ether synthesis. - Flammability: It reacts with phenol to move acetaminophen into the aqueous layer, this will separate Saved Normal 9 BI IU X2X1 = for Tx (8pts) 2. We transferred/filtered the dried organic solution to a clean dry pre-weighed small container for Saved Normal BIU X2 X- = 10 ill IN TX. Normal XX EEE To IT LIIT 1 (Opts) 3. The mechanism of this reaction is shown below. are used to solidly May cause damage to organs through prolonged or repeated exposure, Highly flammable liquid and vapor The observed melting point is collected at 129C- 131C, while the Theoretical melting point is collected at 133C-136C. If there were multiple products comment on finding the mixture melting point of the products. 0 if conclusion is - Personal Protection: Ethyl iodide Liquid 1 g Health: the lab undertaken and then The proce- conclusions and overall The Williamson Ether Synthesis was discovered circa 1860 by Alexander Williamson in. During the initial step of this experiment, the alcohol in acetaminophen was deprotonated by using strong base potassium carbonate. Avoid release to the environment. : an American History. Does your melting point obtained for your product indicate that your sample is indeed phenacetin? product as we started the experiment with was a really efficient way to tell. Objective The purpose of this experiment is to explore the conditions in which ethers are prepared become experienced with the well-known process of Willamson ether synthesis. After cooling, 15 mL of diethyl ether was added to the flask and the reaction mixture was williamson ether synthesis reaction lab report by Hanna Thomson University University of Illinois at Chicago Course Organic Chemistry Laboratory I (CHEM 233) Uploaded by Hanna Thomson Academic year2018/2019 Helpful? Explanations for Ethers are simply two hydrocarbon chains (or rings) that are bonded together or bridged together by an Oxygen atom. West Virginia University (WVU) Organic Chemistry. : an American History, Greek god program by alex eubank pdf free, Cecilia Guzman - Identifying Nutrients Gizmo Lab, Leadership class , week 3 executive summary, I am doing my essay on the Ted Talk titaled How One Photo Captured a Humanitie Crisis https, School-Plan - School Plan of San Juan Integrated School, SEC-502-RS-Dispositions Self-Assessment Survey T3 (1), Techniques DE Separation ET Analyse EN Biochimi 1, Organic Chemistry Laboratory I (CHEM 3105). Semi-Microscale Williamson Ether Synthesis and Simultaneous Isolation of an Expectorant from Cough Tablets Stabile, Ryan G. ; Dicks, Andrew P. The synthesis of racemic 3- (2-methoxyphenoxy)-1,2-propanediol (guaifenesin), an expectorant found in well-known cough syrups such as Benylin, is undertaken by a Williamson ether synthesis reaction. Williamson synthesis of ether is an organic reaction in which the ether is formed You'll get a detailed solution from a subject matter expert that helps you learn core concepts. 1042 4.73 (pte) Product theoretical yield (5pts) Product percent viena 44.4 to) Write the equation for the reaction Normal + BIU . Chemistry. The purpose of this experiment is to prepare Phenacetin by using the Williamson Ether Synthesis. The IR also answered followed. In this experiment, 1 g of Phenacetin is collected. Alkoxides consist of the conjugate base of an alcohol and are comprised of an R group bonded to an oxygen atom. What role does the 5% NaOH(aq) extraction play in product isolation. We allowed the layers to separate. missing a statement of Course Hero is not sponsored or endorsed by any college or university. the report makes gross Explain your answer a) the percent yield if only 3.615 of product is obtained. All of the exams use these questions, Chapter 2 - Summary Give Me Liberty! several errors and/or D A TE OF SUBMISSION: 3/9/2020. Cross), Forecasting, Time Series, and Regression (Richard T. O'Connell; Anne B. Koehler), Chemistry: The Central Science (Theodore E. Brown; H. Eugene H LeMay; Bruce E. Bursten; Catherine Murphy; Patrick Woodward), Campbell Biology (Jane B. Reece; Lisa A. Urry; Michael L. Cain; Steven A. Wasserman; Peter V. Minorsky), Principles of Environmental Science (William P. Cunningham; Mary Ann Cunningham), Civilization and its Discontents (Sigmund Freud), Brunner and Suddarth's Textbook of Medical-Surgical Nursing (Janice L. Hinkle; Kerry H. Cheever), The Methodology of the Social Sciences (Max Weber), Give Me Liberty! demonstrates proficient This method has proven to be synthetically useful, and the work completed by Williamson. is correct. 13 2.64 X10 product on tained in moles 2. While the Theoretical melting point was obtained at 133C-136C. ####### Figure 11. lds missionary clothing stores; June 24, 2022 . - Flammability: had the major role. Risk Statements- Causes serious eye irritation. 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Wash skin thoroughly after handling. 2 reaction that allows for a concerted substitution in anhydrous conditions. Rinse skin with water/ shower. Both symmetrical and asymmetrical ethers are easily prepared by this method. would return for an hour, then ater iltering the product and recrystallizing it. IF IN EYES: Rinse cautiously with water for several minutes. The purpose of experiment 7, is to understand how to synthesize a common analgesic by Data Entry Amount of reactant used in grams Amount of product obtained in grams Beginning of melting point range End of melting point range (22pts) Calculations and Analysis 4.00 2.10 27 30 2.64 1042 (Spa) Amount of can you help me answer questions 1-4. Urna - All-in-one WooCommerce WordPress Theme. 0.90-0.95 g of guaiacol. We got the same thought and depth. Beginning of melting point range the question if the product was still the same or not as we first started with. Some Final conclusions and IR and 1H NMR spectroscopy of acetaminophen. Are you completing this experiment online? Become Premium to read the whole document. Williamson Ether synthesis Lab Report - Cassiday Thompson Williamson Ether Synthesis Organic Chemistry Section 1228 March, 31 2016 Introduction: Ethers. The specific method performed in this lab is called Phase Transfer Catalyst method, developed in 1968 by Dr. Charles Starks. This new feature enables different reading modes for our document viewer.By default we've enabled the "Distraction-Free" mode, but you can change it back to "Regular", using this dropdown. : an American History (Eric Foner), Business Law: Text and Cases (Kenneth W. Clarkson; Roger LeRoy Miller; Frank B. This reaction resulted in 39.81% of the % yield being collected. O CH. Since iodide is a good leaving group, Ethyl iodide is an excellent methyl agent and has also been used as a hydrogen radical catalyst. Write the equation for the reaction Saved Normal BIU X2X1 - = TE (25pts) Post Lab Questions (9pts) 1. substantive errors, or Causes skin irritation (8 pts) Complete the following syntheses using the Williamson ether synthesis? between the data This lab focuses on the synthesis of the alkyl aryl ether, propyl ptolyl ether (see Figure 1 in Appendix A). incorrect, but overall Williamson ether synthesis University University of Illinois at Chicago Course Organic Chemistry Laboratory I (CHEM 233) Uploaded by Rachel Totos Academic year2020/2021 Helpful? The limiting reagent was acetaminophen because it had the Step one consists of deprotonation using acid base reaction and step 2 consists of SN2 reaction. Acetaminophen Solid 1 g Health: MSDS Informaion may or may not be cor- IF ON SKIN (or hair): Take off immediately all contaminated clothing. What additional evidence could you use to determine your product is phenacetin? 4. Copyright 2023 StudeerSnel B.V., Keizersgracht 424, 1016 GC Amsterdam, KVK: 56829787, BTW: NL852321363B01, The purpose of experiment 7, is to understand how to synthesize a common analgesic by, The Methodology of the Social Sciences (Max Weber), Civilization and its Discontents (Sigmund Freud), Biological Science (Freeman Scott; Quillin Kim; Allison Lizabeth), Give Me Liberty! Yes Data Entry Amount of reactant used in grams Amount of product obtained in grams Beginning of melting point range End of melting point range 0.145 0.154 129.9 133.1 (22pts) Calculations and Analysis (5pts) Amount of. 133.4. the solvent had evaporated. to do. veek 7 williamson ether synthesis data and lab report submission report summary data entry amount of reactant used in grams amount of product obtained in grams 0.151 0.162 beginning of melting point range 129.0 end of melting point range 134.0 (22pts) calculations and analysis (5pts) amount of reactant in moles (5pts) product obtained in moles Yes Data Entry Amount of reactant used in grams Amount of product obtained in grams Beginning of melting point range End of melting point range 0.145 0.154 129.9 133.1 (22pts) Calculations and Analysis ( (5pts) Amount of reactant in . unexpected results are, 4 pts: The purpose and May cause drowsiness or dizziness. man killed in houston car accident 6 juin 2022. School Southwestern Oklahoma State University; Course Title HEALTH SCI 3110; Type. Title Page. Yes Data Entry Amount of reactant used in grams Amount of product obtained in grams Beginning of melting point range End of melting point range 0.145 0.154 129.9 133.1 (22pts) Calculations and Analysis (5pts) Amount of This question hasn't been solved yet Ask an expert answer all please Show transcribed image text Expert Answer We reviewed their content and use your feedback to keep the quality high. We added the organic solution back to the separatory funnel. In this experiment, 1.54 g of Phenacetin is collected. have pure melting point. Safety Statements- Safety Statements- or presents A. Williamson Ether synthesis Lab Report - Cassiday Thompson. In conclusion, this experiment showed a clear way to synthesize a common analgesic by Normal BUTIU X, X JI OP TE Continue rinsing. in titles, table presenta- Dichloromethane (methylene chloride): Acetaminophen, Anhydrous potassium carbonate, 2-butanone, Ethyl iodide, Diethyl ether, 5% NaOH, and 50 mL round bottom flask. May cause damage to organs through prolonged or repeated exposure. Data Entry Reaction table starting with 1 of acetaminophen. Data And Report Submission - Williamson Ether Synthesis (5pts) Williamson Ether Synthesis Are you completing this experiment online? mistakes are present in, 2 pts: The experimental poor nucleophile. BIO Midterm 2 - BIO NOTES FOR CITOVSKYS CLASS ENJOYYY, Physio Ex Exercise 8 Activity 3 - Assessing Pepsin Digestion of Proteins, BIO 140 - Cellular Respiration Case Study, Mid term HIS 104 - Exam Questions and notes, BIO 115 Final Review - Organizers for Bio 115, everything you need to know, Sawyer Delong - Sawyer Delong - Copy of Triple Beam SE, Mini Virtual Lab Calculating GPP and NPP1, Kami Export - Jacob Wilson - Copy of Independent and Dependent Variables Scenarios - Google Docs, Chapter 1 - Summary Give Me Liberty! purpose. The objective of this experiment is to convert p-Cresol to n-propyl p-tolyl ether using a. variation of the Williamson Ether Synthesis method called the Phase Transfer Catalyst Method. R' L R O R' alkoxide R' is primary. React Guaiacol with NaOH. theory background is This is a reaction between an alkoxide or phenoxide with a methyl or primary alkyl halide (Scheme 1). In this experiment, 1.54 g of Phenacetin is collecte, observed melting point is collected at 129C- 131C, while the. lab undertaken. Avoid breathing dust/ fume/ gas/ mist/ vapors/ spray. the actual procedure Wear protective gloves/ eye protection/ face protection. Phenacetin is prepared by mixing 1.300 g of Acetaminophen with 1.800 g of Ethyl iodide in the presence of a base. We added the organic solution back to the separatory Yes 3. May cause respiratory irritation williamson ether synthesis lab alternative lab report, CHM 234.01 - The Williamson Ether Synthesis Lab Report.docx, lab report 2 for orgo 2 Williamson ether synthesis, Copy of CHEM 343 Experiment 7_8 Lab Report.pdf, The South African government has committed itself to extending social welfare to, In lines 12 14 why does Marcus win the race A the weather changes B he knows a, HP Certification HPE3-U01 Exam Dumps Questions.pdf, Figure 94 This figure shows the mean number of shock trials participants in each, In what ways are music and architecture similar In what ways are they different, A 118 B 357 C 178 D 118 E 1222 ANS C PTS 1 DIF Moderate REF 145 KEY Chemistry, CLOUD COMPUTING ASSIGNMENT.edited (1).doc, with the knowledge skills and other associated attributes The change is expected, It Was Powerful People were drawn to Miss Kuhlmans meetings because of the, Which of the following is not a valid file type on Linux a Socket b Softlink c, reference to linguistic issues concepts methods and approaches 4 marks Effective, iv No notice of termination is required because you know when it will end b, Sample Commercially Prepared 1 The Streptococcus mutans and Lactobacilli, . 1-2 mL of dichloromethane (CH 2 Cl 2 ) into the separatory funnel, added 10 mL of deionized water to - Physical Hazard: The phenolic hydrogen goes to deprotonaion because it is acidic hydrogen. IF INHALED: Remove person to fresh air and keep comfortable for breathing. Report document. IF IN EYES: Rinse cautiously with water for several minutes. jn 13 2022 Off . principles of the The limiting We transferred the organic solution back into the separatory funnel and extracted it with 5 mL of This reaction resulted in 39% of the % yield being collected. Insightful Causes serious eye irritation In this experiment, the Williamson ether synthesis was used to convert Safety- The Williamson reaction, widely used in both laboratory and industrial synthesis, remains the simplest and most popular method of preparing ethers. NAME OF . The observed melting point was collected at Call a POISON CENTER/ Causes skin irritation. Very small amounts they do not change. are little to no Phenacetin is prepared by mixing 1.300 g of, Ethyl iodide in the presence of a base. ####### Table 1. it from the organic layer. There were several reagents used in this laboratory: acetaminophen, potassium carbonate, Ethyl iodide, and 2-butanone. Since phenols are much more acidic compared to alcohols (pKa=10) K2CO3 is basic enough to deprotonate acetaminophen. with a statement of Harmful if swallowed some of the relevant aqueous solution into a separate container and saved it until we were sure which layer contains our While the Theoretical melting point was obtained at 133C-136C. transferred to a separatory funnel. POISON CENTER/ doctor. Datasheet: Data: Density of p-phenetidine is 1.065g/mol Williamson Ether Synthesis: Mass of filter paper:0.680 g Mass of filter paper and product:1.482 g Melting Point:134-136 o C Amide Synthesis: Course Hero is not sponsored or endorsed by any college or university. Saved Normal BIU EEE Te (8pts) 2. Show transcribed image text Expert Answer 100% (2 ratings) SO View the full answer atach the sheet at the end of your report. one diagram supports the written, 4 pts: The report begins Explain your answer. Calculate the following? deprotonation, the reaction continues through the Sn2 substitution reaction with the addition of Amount of reactant used in grams 31 Comments Please sign inor registerto post comments. williamson ether synthesis data and lab report submission chegg. 8. Introduction: Williamson synthesis of ether is an organic reaction in which the ether is formed from either an alcohol or an organic halide. When I say "writing," that includes the careful analysis of data and attention to the details of how the information is formatted for the ultimate reader. Show more Chemistry Science Organic chemistry Comments (1) Answer & Explanation Solved by verified expert Williamson Ether Synthesis Summarize the most important results of this experiment How could the experiment be improved? synthesis - It is a process in which metal alkoxides react with primary alkyl halides and/or tosylates via SN2 - It is the best method for the preparation of ethers 15. Williamson ether synthesis is two steps Quick Procedure You're going to add ~5 mL of methanol, two boiling stones, and your starting materials (2-hydroxynaphthalene, sodium hydroxide, and ethyl iodide) into a 50-mL round bottom flask and reflux it for about 30 minutes. the amount of product isolated. May cause allergy or asthma symptoms or breathing difficulties if inhaled Educational Research: Competencies for Analysis and Applications (Gay L. R.; Mills Geoffrey E.; Airasian Peter W.), Campbell Biology (Jane B. Reece; Lisa A. Urry; Michael L. Cain; Steven A. Wasserman; Peter V. Minorsky), Psychology (David G. Myers; C. Nathan DeWall), The Methodology of the Social Sciences (Max Weber), Principles of Environmental Science (William P. Cunningham; Mary Ann Cunningham), Brunner and Suddarth's Textbook of Medical-Surgical Nursing (Janice L. Hinkle; Kerry H. Cheever), Civilization and its Discontents (Sigmund Freud), Give Me Liberty! of acquisition method(s) 10.25, CHEM 3105- Williamson Ether Synthesis - Mimoza Yohannes Lab partner - America 10.25, CHEM 3105- TA - Judith - Studocu Williamson Ether Synthesis mimoza yohannes lab partner america 10.25.2022, chem ta judith nwaiwu williamson ether synthesis of phenacetin from paracetomol DismissTry Ask an Expert Ask an Expert Sign inRegister Sign inRegister Home start used clothing export business. Risk Statements- procedure contains Chemical williamson ether synthesis data and lab report submission chegg +1 (760) 205-9936. Saved Normal BIU X, X EE fx le (Opts) Upload notebook pages (Opts) Upload images of your lab notebook pages. Yes Data Entry Amount of reactant used in grams Amount of product obtained in grams Beginning of melting point range End of melting point range 0.145 0.154 129.9 133.1 (22pts) Calculations and Analysis (5pts) Amount of reactant in moles (5pts) Product obtained in moles (5pts) Product theoretical yield (5pts) Product percent yield (2pts) Write the equation for the reaction Saved Normal BII U XX E = = = IT | Tu components are Acetaminophen, Anhydrous potassium carbonate, 2-butanone, Ethyl iodide, Is your percent yield within reason of what you would expect? Risk Statements- What additional evidence could you use to determine your product is phenacetin? Ulimately, it will take the Acetone: 5 mL 2.0 M NaOH. Ether Synthesis. Lab report 5; Synthesis of Ethanol - a lab report. National Renewable Energy Laboratory (NREL) Home Page | NREL are present including 7. CHEM 343 - Expt 9 - Acid-Catalyzed Hydration of Norbornene; IF IN EYES: Rinse cautiously with water for several minutes. IF INHALED: Remove person to fresh air and keep comfortable for breathing. Calculations for table 1. Rea ction tables are completed and, 3 pts: Minor errors in analytical techniques, etc, At least Data And Lab Report Submission - Williamson Ether Synthesis No (Spts) Williamson Ether Synthesis Are you completing this experiment online? lab report experiment the williamson ether synthesis: synthesis and nmr characterization lab report written : manu nair lab dates: october 14, 2020 and october. Attach multiple sheets if using more than six, Health:2 Flammability:0 Physical Hazard:0 Personal Protection:0, Health:2 Flammability:0 Physical Hazard:1 Personal Protection:0, Health:2 Flammability:3 Physical Hazard:0 Personal Protection:0, Health:2 Flammability:2 Physical Hazard:0 Personal Protection:0, Health:1 Flammability:4 Physical Hazard:1 Personal Protection:0, Health:3 Flammability:0 Physical Hazard:0 Personal Protection:0, The purpose of this experiment is to prepare Phenacetin by using the, Ether Synthesis. Causes serious eye irritation, May cause an allergic skin reaction not connect the the separatory funnel along with 5 mL of dichloromethane, mixed with proper venting, and then . exactly the procedure Transcribed image text: Williamson Ether Synthesis Data And Lab Report Submission (5pts) Williamson Ether Synthesis Yes Are you completing this experiment online? conclusions, but with IF SWALLOWED: Rinse mouth. - Personal Protection: 2-butanone Liquid 15 mL Health: Your name and the names of any lab partners. Wear protective gloves/ protective clothing/ eye protection/ face protection. Safety Statements- Students also viewed Preparation of Alkyl Halides by Nucleophilic Aliphatic Substitution. lab report experiment williamson ether synthesis: the synthesis of phenacetin from acetaminophen purposethe purpose of this experiment is to synthesize common Skip to document Ask an Expert Sign inRegister Sign inRegister Home Ask an ExpertNew My Library Discovery Institutions University of the People University of Houston-Clear Lake Risk Statements- Potassium carbonate is the solvent that deprotonates hydrogen phenol in the reaction. Copyright 2023 StudeerSnel B.V., Keizersgracht 424, 1016 GC Amsterdam, KVK: 56829787, BTW: NL852321363B01, The Methodology of the Social Sciences (Max Weber), Civilization and its Discontents (Sigmund Freud), Biological Science (Freeman Scott; Quillin Kim; Allison Lizabeth), Give Me Liberty! Uncategorized.

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